摘要
以1,1,2,2-四(4-溴苯基)乙烯为原料,通过氰基取代、Suzuki反应,以及Sharpless反应,得到两种基于四苯乙烯核心的四氮唑衍生物,并通过1HNMR,13CNMR,IR,MS对其结构进行验证.通过固体荧光测试发现,这两个化合物具有良好的荧光性质.
Two tetraphenylethylene tetrazole compounds were synthesized through cyano substitution,Suzuki reaction and Sharpless reaction. The structures of two compounds were testified by1 HNMR,13 CNMR,IR and MS.Based on the fluorescence analysis,it was found that these two compounds had remarkable fluorescence properties.
作者
周磊
周泽宇
汪芳明
ZHOU Lei;ZHOU Zeyu;WANG Fangming(School of Environmental and Chenfical Engineering,Jiangsu University of Science and Technology,Zhenjiang 212003,China)
出处
《江苏科技大学学报(自然科学版)》
CAS
2018年第3期426-430,共5页
Journal of Jiangsu University of Science and Technology:Natural Science Edition
基金
江苏科技大学博士启动基金
江苏科技大学自然基金预研项目
关键词
四苯乙烯
四氮唑衍生物
荧光性质
tetraphenylethylene
tetrazole derivatives
fluorescence property