QuickPress高温高压设备的改进与温度标定

Improvement and Temperature Calibration of QuickPress High Temperature and High Pressure Equipment

QuickPress活塞圆筒装置样品装填难度大,耗材价格高.本文自主设计并加工出一套该装置的样品仓装填耗材,具有装样操作简单快捷,耗材价格低廉等特点,适用于导体材料、腐蚀性材料、氧化物材料等样品的高温高压实验.温度标定后使用该套耗材进行高温高压实验时,不需要安装热电偶,根据加热功率即可确定样品加热温度,可进一步简化实验操作流程、节省实验时间.

For QuickPress piston-cylinder device,Sample loading is very difficult,and the consumptive materials are very expensive.A set of sample storehouse filling materials designed in this paper is cheap,convenient for loading,and suitable for conducting materials,corrosive materials,oxide materials and others in high temperature and high pressure experiment.After temperature calibration,it will be no longer need the thermocouple,and the operation process will be simplified.The temperature of the sample can be calculated according to the heating power.