摘要
对1-烯丙基-3-丁基咪唑氯离子液体的合成进行了研究,考察1-烯丙基-3-丁基咪唑氯的反应条件对产品收率的影响,并通过红外光谱和核磁共振光谱进行了表征。实验结果表明:在n(烯丙基氯)∶n(N-丁基咪唑)=1.3∶1,反应时间为3 h,反应温度为50℃的条件下离子液体收率最高,可达到93.64%。
The synthesis of 1-allyl-3-butylimidazolium chloride ionic liquid was studied. The influence of reaction conditions of 1-allyl-3-butylimidazolium chloride on the yield of products was investigated,and characterized by IR and NMR spectroscopy. The experimental results show that the yield is the highest when the n（ allyl chloride） ： n（ N-butyl imidazole）= 1. 3∶ 1,reaction time is 3 h,and the reaction temperature is 50 degrees. The yield is 93. 64 %.
作者
张玲玲
马瑞
刘雁红
Zhang Lingling 1,2 ,Ma Rui 1,2 ,Liu Yanhong 1,2(1.Tianjin University of Science and Technology, Institute for New Rural Development,Tianjin 300457,China;2.College of Food Engineering and Biotechnology,Tianjin University of Science ＆ Technology,Tianjin 300457,Chin)
出处
《山东化工》
CAS
2018年第14期5-8,共4页
Shandong Chemical Industry
基金
天津科技大学新农村发展研究院开放基金资助项目(项目编号:xnc201603)
关键词
离子液体
绿色溶剂
合成
表征
ionic liquids
green solvent
synthesis
characterization
