4’-(4-溴萘-1-基)[1,1’-联苯基]-4-腈的合成与表征

Synthesis and Characterization of the 4'-(4-Bromonaphthalene-1-yl)[1,1'-Biphenyl]-4-Nitrile

以4-溴苯腈为起始原料经过Miyanra硼化反应、Suzuki偶联反应和溴化反应等合成了4’-(4-溴萘-1-基)[1,1’-联苯基]-4-腈.通过~1H NMR、^(13)C NMR表征了化合物的结构,通过TG、荧光发射光谱等研究了标题化合物的发光效率和稳定性.

4’-（4-Bromonaphthalene-1-yl）[1,1’-biphenyl]-4-nitrile was synthesized by Miyanra reaction,Suzuki reaction and bromination reaction by using 4-bromobenzonitrile as a raw material in this paper. The structureof synthesized compound was characterized by 1H NMR and 13C NMR. Thermal properties and optical properties ofthe title compound were determined with TG and fluorescence spectrum.