摘要
利用溶剂热合成法制备金属有机骨架材料MIL-53(Fe)。通过X射线衍射仪(XRD)、电子扫描电镜(SEM)、傅立叶变换红外光谱仪(FTIR)表征手段对材料的晶相结构及组成成分进行分析。常温常压下,通过催化还原对硝基苯酚的反应考察MIL-53(Fe)的催化活性。结果表明,MIL-53(Fe)的催化活性良好,5min对硝基苯酚的转化率达到96.8%。
In this paper,MIL-53(Fe) was prepared by sol thermal method.The structure and composi tion of sample was characterized by means of X ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transformation infrared spectrometer (FTIR).Catalytic activity of sample was investi gated by catalytic reduction of p nitrophenol at ambient temperature and pressure.The results showed that MIL- 53 (Fe)existed good catalytic performance and the conversion of p nitrophenol reached 96.8% in five minutes.
作者
杨宇珩
张丹
孟秀红
段林海
YANG Yuheng;ZHANG Dan;MENG Xiuhong;DUAN Linhai(School of Chemistry and Materials Science,Liaoning Shihua University,Fushun 113001,China)
出处
《化工科技》
CAS
2018年第5期5-8,共4页
Science & Technology in Chemical Industry
基金
国家自然科学基金面上项目(21476101)
辽宁省教育厅项目(L2015304)