天麻酒质量标准研究

Study on Quality Standard of Tianma Health Wine

目的:建立天麻酒的质量控制方法,为其产品的质量控制提供依据。方法:对酒中药材天麻、五味子、酸枣仁建立薄层色谱定性鉴别方法研究,对天麻素进行高效液相定量测定方法研究。结果:薄层色谱法能检出天麻、五味子、酸枣仁;当天麻素进样量在0. 131~1. 835μg范围内与峰面积值呈良好的线性关系(r=0. 9999),平均回收率为98. 5%,RSD为2. 4%。结论:所建立的方法专属性强、准确、方便,可用以控制天麻酒的质量。

Objective： To establish the quality control method of Tianma Health Wine and provide the basis for controlling the product quality. Methods： Rhizoma gastrodiae,schisandra chinensis,and spine date seed in Tianma health wine were qualitatively identified by TLC,and the content of gastodin was determined by HPLC. Results： Rhizoma gastrodiae,schisandra chinensis and spine date seed in Tianma Health Wine could be detected by TLC; The sample quantity of gastrodin within the concentration range of 0. 131 - 1. 835μg had good linear relationship with the peak area（ R = 0. 9999）,and the average recovery rate of gastrodin was 98. 5%（ RSD = 2. 4%）. Conclusion： The established methods of quality standard of Tianma Health Wine are of good specialization,accuracy and simplicity,which can be used to control the quality of theproduct.