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多弧离子法制备的Ti(C,N)微结构随C<sub>2</sub>H<sub>2</sub>/N<sub>2</sub>流量比变化的研究(英文)

STUDY OF THE MICROSTRUCTURE OF TI(C,N) FILM PREPARED BY MULTI-ARC ION-PLATING
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摘要 用多弧离子法在高速钢(W18Cr4V)基底上沉积了Ti(N,C)薄膜,并运用SEM、XRD、XPS对该膜微观结构随进气流量比r=C<sub>2</sub>H<sub>2</sub>/N<sub>2</sub>变化的情况进行了测试和分析。结果表明薄膜随r增加趋于致密,在r值较小时呈现较强的(111)择优取向,随着r值增大,(111)这一取向逐渐变弱,(220)取向渐强,薄膜呈现典型面心立方结构,主要成分为复合相Ti(N,C),膜含有少量石墨相成分存在。 The Ti (C, N) multi-component coatings are deposited on the HSS steel (W18Cr4V) substrates by muti - arc ion - plating with variationg of reactive gas flow ratio r=C2H2/N2, and the coatings are tested and analysed by XPS, XRD , SEM techniques , The results show that the Ti ( C, N ) coating exhibits a very-strong (111) preferred orientation when the value of r is very low. The (111) peak decreases and (220) peak increases with the increasing of r while the coating becomes more dense . The film shows typical face - centered cubic structure . The component of the film is Ti ( C, N), but there is little graphite component in the coating.
出处 《苏州大学学报(自然科学版)》 CAS 1997年第2期81-85,共页 Journal of Soochow University(Natural Science Edition)
关键词 多弧离子法 择优取向 SEM XRD XPS Mud - arc ion - plating preferred orientation SEM XRD XPS.
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