Synthesis and Crystal Structure of N-(5-Phenylseleno)pentyl Succinimide

Synthesis and Crystal Structure of N-(5-Phenylseleno)pentyl Succinimide

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摘要 N-(5-phenylseleno)pentyl succinimide 1, C15H19NO2Se (Mr = 324.27), was prepared by treating Br(CH2)5SePh with potassium succinimide. Its crystal structure has been determined by X-ray single-crystal diffraction. The crystal of 1 belongs to monoclinic system, space group P21/c with the crystal cell parameters: a = 18.018(6), b = 5.980(2), c = 14.682(5) ? = 109.977(6)? V = 1486.7(9) 3, Z = 4, Dc = 1.449 g/cm3, (MoK? = 2.523 mm-1, F(000) = 664,the final R = 0.0302 and wR = 0.0666 for 2623 independent observed reflections with I > 2(I). Structure analyses revealed that there exist strong nonclassical hydrogen bonds (CH…O).

作者张万轩于海涛等

机构地区 DepartmentofChemistry

出处《Chinese Journal of Structural Chemistry》 SCIE CAS CSCD 北大核心 2002年第5期517-519,共3页 结构化学（英文）

基金 This work was supported by the NNSFC (No. 29832030)

关键词 N-(5-phenylseleno)pentyl succinimide PREPARATION crystal structure N-(5-苯基硒基)戊烷基琥珀酰亚胺合成晶体结构 C15H19NO2Se

分类号 O626 [理学—有机化学]

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Chinese Journal of Structural Chemistry

2002年第5期

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Synthesis and Crystal Structure of N-(5-Phenylseleno)pentyl Succinimide

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