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微波合成半导体CuS纳米粒子和Bi_2S_3纳米棒 被引量：2

Preparation of semiconductor CuS nanoparticles and Bi_2S_3 nanorods by microwave irradiation
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摘要 在甲醛溶液中 ,以 Cu(Ac) 2 、Bi(NO3) 3和 TAA为源材料 ,通过微波加热合成了 Cu S半导体纳米粒子和 Bi2 S3纳米棒 ,并用 XRD。 CuS nanoparticles of ca. 7 nm in size have been successfully prepared by a very simple fast reaction between copper acetate and thioacetamide (TAA) in a formaldehyde solution using microwave irradiation. Bi 2S 3 nanorods with a diameter of ca. 50 nm and a length of up to ca. 2 μm also have been successfully prepared from a formaldehyde solution of bismuth nitrate and thioacetamide (TAA) by microwave irradiation. Powder X ray diffraction (XRD) patterns indicates that the products are pure orthorhombic Bi 2S 3 phase, Hexagonal phase CuS, respectively. The products were characterized by the techniques of transmission electron microscopy (TEM).
作者 廖学红 郑坚
机构地区 黄冈师范学院化学系 黄冈师范学院生物系
出处 《黄冈师范学院学报》 2002年第6期26-27,共2页 Journal of Huanggang Normal University
基金 湖北省教育厅科学研究青年项目基金 (No.2 0 0 1B43 0 0 1)资助
关键词 微波辐射 合成 CuS纳米粒子 Bi2S3纳米棒 半导体 纳米材料 制备 preparation CuS nanoparticles Bi 2S 3 nanorods Semiconductor microwave irradiation
分类号 TB383 [一般工业技术—材料科学与工程]
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参考文献6

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二级参考文献28

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共引文献10

同被引文献30

  • 1吕维忠,刘波,韦少慧,游新奎,李均钦.纳米硫化铜的超声波化学合成及其表征[J].电子元件与材料,2004,23(10):4-5. 被引量：12
  • 2台玉萍,李宏涛.非水溶剂法制备纳米硫化铜微粉[J].长春工业大学学报,2007,28(1):22-25. 被引量：4
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引证文献2

二级引证文献8

黄冈师范学院学报
2002年 第6期

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