摘要
Effects of solid solution treatment and cooling on the morphology of long period stacking order(LPSO)phase and precipitation hardening behavior of Mg?2Dy?0.5Ni(molar fraction,%)alloy were investigated.Microstructures of the as-cast alloy mainly consisted ofα-Mg phase,bamboo-like Mg12DyNi phase with LPSO structure distributed between dendrites and small amounts of cubic Dy phases.During solid solution treatment at565oC for12h and subsequent different cooling conditions,dot-shaped,block,fine lamellar and rod-shaped LPSO phases precipitate in Mg matrix,respectively.For continuous cooling conditions(furnace and air cooling),the fine lamellar LPSO phase generally forms in grain interior and its volume fraction increases and block LPSO phase coarsens with increasing cooling time.For discontinuous cooling conditions(air cooling after furnace cooling to415and265°C),the dot-shaped LPSO grows into the rod-shaped phase,which results in an decrease of cooling hardening behavior of alloy.
研究了固溶和冷却处理对Mg-2Dy-0.5Ni(摩尔分数,%)合金中的长程堆垛有序(LPSO)相形貌及析出硬化行为的影响。铸态合金组织主要包括α-Mg相、分布在枝晶间具有LPSO结构的竹尖状Mg_(12)DyNi相和少量立方体状的Dy相。在565℃固溶处理12 h及随后不同的冷却过程中,点状、块状、细薄片状和棒状的LPSO相分别在基体中析出。在连续冷却(空冷和炉冷)的条件下,细薄片状的LPSO相逐渐在晶粒内部析出;随着冷却时间的延长,其体积分数亦增加,且块状的LPSO相发生粗化。在不连续冷却(炉冷到415℃+空冷和炉冷到265℃+空冷)条件下,点状LPSO相生长成棒状相,降低了合金的冷却硬化作用。
基金
Projects(51301082,51464031) supported by the National Natural Science Foundation of China
Project(2015011038) supported by the Natural Science Foundation of Shanxi Province,China