摘要
目的:建立花椒中柠檬烯、芳樟醇含量快速灵敏的检测方法,同时为陇南大红袍花椒的质量控制提供研究方法。方法:采用水蒸气蒸馏法提取陇南大红袍花椒挥发油,以正己烷为稀释剂,用气相色谱-质谱法分析其柠檬烯、芳樟醇。结果:甘肃陇南大红袍花椒中柠檬烯含量为0.37%±0.04%,芳樟醇含量为1.07%±0.16%。结论:本文建立的GC-MS方法,具有灵敏、快速、准确的特点,可供甘肃陇南大红袍花椒质量控制及化学成分含量测定。
Objective:To establish a rapid and sensitive detection method for the determination of limonene and linalool in Zanthoxylum bungeanum,and provide a research method for the quality control of Dahongpao Z.bungeanum in Longnan.Methods:The volatile oil of Dahongpao Z.bungeanum in Longnan was extracted by steam distillation.And it’s limonene and linalool were analyzed by gas chromatography-mass.Hexane is used as a thinner.Results:The content of limonene in Dahongpao Z.bungeanum was 0.37%±0.04%,and the content of linalool is 1.07%±0.16%.Conclusion:The GC-MS method established in this paper is sensitive,rapid and accurate,and can be used for the quality control and chemical composition determination of Dahongpao Z.bungeanum in Longnan.
作者
司昕蕾
蔡秀荣
曹瑞
边甜甜
辛二旦
牛江涛
张爱霞
李越峰
SI Xin-lei;CAI Xiu-rong;CAO Rui;BIAN Tian-tian;XIN Er-dan;NIU Jiang-tao;ZHANG Ai-xia;LI Yue-feng(University of Traditional Chinese Medicine of Gansu,Lanzhou 730000,China;Key laboratory of standard and quality of Chinese medicine research of Gansu,Lanzhou 730000,China;Lanzhou Foci Pharmacognostical Co.,Ltd.,Lanzhou 734000,China)
出处
《中国现代中药》
CAS
2019年第2期173-175,193,共4页
Modern Chinese Medicine
基金
国家自然科学基金资助项目(81460611)
国家教育部科学技术研究重点基金资助项目(212186)
甘肃省自然科学基金资助项目(2010:1010RJZA212
2014:145RJZA076)
甘肃省财政厅高校基本科研业务费专项基金资金项目(2013-2)
兰州市科技局项目(2014-1-188)
甘肃省中医药管理局科研课题(GZK-2015-57)
自然科学基金创新基地和人才计划项目(18JR3RA197)
2018年度甘肃省中药质量与标准研究重点实验室开放基金(ZYZL18-008)
甘肃中医药大学研究生创新基金(CX2018-27)
关键词
甘肃陇南大红袍花椒
柠檬烯
芳樟醇
气相色谱-质谱法
Dahongpao Zanthoxylum bungeanum in Longnan
limonene
linalool
gas chromatography-mass spectrometry
