期刊文献+

2-吡啶酮肟的合成

下载PDF
导出
摘要 试验了不同反应条件下合成2-吡啶酮肟的产率,从而确定了合成目标产物的最佳条件。通过试验确定最佳反应条件为:室温反应6 h,调pH=6,产率可达84.8%。
出处 《长治学院学报》 2018年第5期46-47,共2页 Journal of Changzhi University
基金 国家自然科学青年基金(21701078)
  • 相关文献

参考文献2

二级参考文献9

  • 1Theocharis C. Stamatatos, Aidan Bell, Paul Cooper, Aris Terzis. Old ligands with new coordination chemistry: Linear trinuelear mixed oxidation state cobalt(Ⅲ/Ⅱ/Ⅲ) complexes and their mononuclear ' ligand' cobalt (Ⅲ) complexes featuring 2-pyridyloximates[J]. Inorg. Chem. Commun,2005(8):533-538.
  • 2X. M. Ren ,Y. C. Chen ,C. He and S. Gao. Spontaneous Magnetization Below7.7 K Basedonan Extended 3-D H-Bonding Network Material;Synthesis ,Crystal Structureand Magnetic Properties[J]. J . C. S. Dalton Trans. ,2002(3):915- 918.
  • 3Constantinos J. Milios, Stergios Piligkos, Aidan R. Bell. A rare mixed-valence state manganese(Ⅱ/Ⅳ) tetranuelear cage formed using phenyl 2-pyridyl ketone oxime and azide as ligands[J]. Inorg. Chem. Commun,2006(9) :638 - 641.
  • 4G. H Wu and D. Y. Wu. Chlorido (pyridine- 2 - carbaldehydeoximato- κ2N, N' ) ( pyridine- 2 - carbaldehydeoxime-κ2N, N') copper(Ⅱ)[J].Acta Cryst. ,2008(E64):m828.
  • 5G. M. Sheldrick :SHELXL297. Program for the Refinement of Crystal Structure[M]. University of Gt -Otingen ,Germany ,1997.
  • 6Dosanjh A, Ikonen T, Wan B, et al. Pirfenidone: A Novel Anti-fibrotic Agent and Progressive Chronic Allograft Rejection[J].Pulm Pharmacol Ther,2002,15(5):433-437.
  • 7Kraus Helmut, Klausener Alexander,Fuerstenwerth Hauke. Process for the Preparation of 2-Substituted 5-Alkyl-pyridine[P].US 5 420 284,1995.
  • 8Hartmann Ludwig A, Stephen John F. Synthesis of 2-Substituted-5-methyl-pyridines[P].US 4 473 696,1984.
  • 9Stephen John Fergus, Hartmann Ludwig A. Synthesis of 2-Substituted-5-methylpyridines from Methylcyclo-butanecarbonitrile, Valeronitrile and Pentenonitrile Intermediates[P].EP 0 162 464,1985.

共引文献3

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部