摘要
为了对铜导线熔痕的Raman光谱鉴定方法进行优化,选择表面无损检测、Raman面成像检测、附着碳洗脱检测三种Raman光谱法对铜导线熔痕进行检测,选择最佳的检测方法,并对检测条件进行优化。实验结果表明:附着碳洗脱检测法是最佳的铜导线熔痕Raman光谱鉴定方法。该方法高效,预处理程序简便,所需的样品用量与放置时间等都满足火灾物证鉴定工作的需求。
In order to optimize the copper wire sintering identification method based on Raman spectroscopy, 3 kinds of Raman spectroscopy method in eluding surface nondestructive testing, Rama n surface imaging detecti on and adhere nt carbo n elution detection were chosen to test the copper wire sintering, choose the best test method, and optimize the test condition. Test results showed that, adherent carbon elution detaction is the best copper wire sintering idenlificalion method based on Raman spectroscopy. The method has high efficiency, simple and convenient preprocessing program, and the sample consumption and storage time required can satisfy the fire physical evidence identification need.
作者
杨涵
汪箭
张健
刘纪达
王志
YANG Han;WANG Jian;ZHANG Jian;LIU Ji-da;WANG Zhi(Hangzhou Fire Detachment. Zhejiang Hangzhou 310016,China;State Key Laboratory of Fire Science, University of Science and Technology of China, Anhui Hefei 230026. China;China People's Police University, Hebei Langfang 065000, China;Daqing Fire Detachment, Heilongjiang Daqing 163000, China)
出处
《消防科学与技术》
CAS
北大核心
2019年第2期211-214,共4页
Fire Science and Technology
基金
国家重点研发计划项目(2018YFC0809502)
关键词
熔痕
RAMAN光谱
表面无损法
Raman面成像
附着碳洗脱法
火灾调查
sin tering
Rama n spectroscopy
surface non destructive testi ng
Raman surface imagi ng
adhere nt carbon elutio n
fire investigation