摘要
Local crystallographic orientation characteristics of grains with different sizes in a ZrTiAlValloy after interrupted cooling from βphase region are investigated by electron backscatter diffraction(EBSD) technique. A statistical analysis of EBSD data shows that bigger parent β grains present weaker variant selection than smaller grains. The relevant influences are studied by comparing the nucleation behavior of grain boundary α(GBα) and succedent growth stage in varisized grains. In-depth analysis indicates that the deviation between pole of GBα and common pole of adjacent parent β grains is responsible for the smaller degree of variant selection inside the bigger parent β grains. The formation of more than one GBα type at the β/β grain boundary with common pole in bigger grains results in obstructing each other for these variants during the following growth stage, while only one type of GBα nucleate at the β/β grain boundary with common pole in smaller grains and it can freely grow into the interior of the grains, leading to stronger variant selection in smaller β grains.
Local crystallographic orientation characteristics of grains with different sizes in a ZrTiAlValloy after interrupted cooling from βphase region are investigated by electron backscatter diffraction(EBSD) technique. A statistical analysis of EBSD data shows that bigger parent β grains present weaker variant selection than smaller grains. The relevant influences are studied by comparing the nucleation behavior of grain boundary α(GBα) and succedent growth stage in varisized grains. In-depth analysis indicates that the deviation between pole of GBα and common pole of adjacent parent β grains is responsible for the smaller degree of variant selection inside the bigger parent β grains. The formation of more than one GBα type at the β/β grain boundary with common pole in bigger grains results in obstructing each other for these variants during the following growth stage, while only one type of GBα nucleate at the β/β grain boundary with common pole in smaller grains and it can freely grow into the interior of the grains, leading to stronger variant selection in smaller β grains.
基金
supported by the National Natural Science Foundation of China(Grant Nos.51531005,51571174&51421001)
the Fundamental Research Funds for the Central Universities(Grant No.106112017CDJQJ138803)
the National Science Foundation for Distinguished Young Scholars of Hebei Province of China(Grant No.E2016203376)
the Hundred Excellent Innovative Talents Support Program in Hebei Province(Grant No.SLRC2017056)