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Effect of tempering temperature on the microstructure and properties of ultrahigh-strength stainless steel 被引量:11

Effect of tempering temperature on the microstructure and properties of ultrahigh-strength stainless steel
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摘要 The microstructure, precipitation and mechanical properties of Ferrium S53 steel, a secondary hardening ultrahigh-strength stainless steel with 10% Cr developed by QuesTek Innovations LLC, upon tem pering were studied by scanning electron microscopy (SEM), transm ission electron microscopy (TEM), X-ray diffraction (XRD), and tensile and impact tests. Based on these results, the influence of the tem pering temperature on the microstructure and properties was discussed. The results show th at decom position occurred when the retained austenite was tem pered above 440 ℃ and that the hardening peak at 482 ℃ was caused by the joint strengthening of the precipitates and martensite transformation. Due to the high Cr content, the trigonal M7C3 carbide precipitated w hen the steel was tem pered at 400 ℃, and M7C3 and M2C (5 -10 nm in size) coexisted w hen it was tem pered at 482 ℃. When the steel was tem pered at 630 ℃, M2C and M23C6 carbides precipitated, and the sizes w ere greater than 50 nm and 500 nm, respectively, but no M7C3 carbide formed. When the tempering tem perature was above 540 ℃, austenitization and large-size precipitates w ere the main factors affecting the strength and toughness. The microstructure, precipitation and mechanical properties of Ferrium S53 steel, a secondary hardening ultrahigh-strength stainless steel with 10% Cr developed by QuesTek Innovations LLC, upon tempering were studied by scanning electron microscopy(SEM), transmission electron microscopy(TEM), X-ray diffraction(XRD), and tensile and impact tests. Based on these results, the influence of the tempering temperature on the microstructure and properties was discussed. The results show that decomposition occurred when the retained austenite was tempered above 440℃ and that the hardening peak at 482℃ was caused by the joint strengthening of the precipitates and martensite transformation. Due to the high Cr content, the trigonal M7C3 carbide precipitated when the steel was tempered at 400℃, and M7C3 and M2C(5–10 nm in size) coexisted when it was tempered at 482℃. When the steel was tempered at 630℃,M2C and M23C6 carbides precipitated, and the sizes were greater than 50 nm and 500 nm, respectively,but no M7C3 carbide formed. When the tempering temperature was above 540℃, austenitization and large-size precipitates were the main factors affecting the strength and toughness.
出处 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2019年第7期1240-1249,共10页 材料科学技术(英文版)
基金 supported financially by the National Natural Science Foundation of China (Nos. 51874081 and 51574063) the Fundamental Research Funds for the Central Universities (Nos. N152306001 and N150204012)
关键词 Age HARDENING AUSTENITE PRECIPITATION TEMPERING Strengthening mechanism M7C3 Age hardening Austenite Precipitation Tempering Strengthening mechanism M7C3
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