摘要
以芳香胺和CS2为原料,在碱性和蒙脱土负载碘作为催化剂的条件下,使用超声辅助制备异硫氰酸酯。实验研究了溶剂、碱性条件、碱的用量、催化剂的用量、反应时间等对异硫氰酸酯收率的影响。
Isothiocyanate was prepared from aromatic amine and CS 2 as raw materials under the conditions of alkaline and montmorillonite supported iodine as catalyst.The effects of solvent,basic conditions,amount of base,amount of catalyst and reaction time on the yield of isothiocyanate were investigated experimentally.
作者
张思
李航
吴会敏
郑兴莉
尹晓刚
Zhang Si;Li Hang;Wu Huimin;Zheng Xingli;Yin Xiaogang(School of Chemistry and Materials Science,Guizhou Normal University,Guizhou Key Laboratory of Functional Materials Chemistry,Guiyang550001,China)
出处
《山东化工》
CAS
2019年第16期7-8,共2页
Shandong Chemical Industry
基金
贵州省大学生创新创业训练计划项目,201810663023号
关键词
异硫氰酸酯
催化
蒙脱土负载碘
超声
isothiocyanate
catalysis
montmorillonite loadingiodine ultrasound assisted
