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Mechanical Properties of Micro-regions in Cement-based Material based on the PeakForce QNM Mode of AFM 被引量:3

Mechanical Properties of Micro-regions in Cement-based Material based on the PeakForce QNM Mode of AFM
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摘要 In this paper, the cement paste and the mortar were tested using the PF-QNM technique. It is shown that the PF-QNM technique is very powerful to characterize the mechanical properties of micro-and nanostructures in the cement-based materials. It does not have strict requirements for test environment and it does not damage the surface of the material. High-resolution images can be obtained very easily, and they can be analyzed statistically. The test results show that PF-QNM analysis can test not only the mechanical properties of the cement paste, but also investigate the interfacial regions in the cement-based material, including the variation in the mechanical properties of interface regions and the extension of the interfacial regions. During the test, care must be taken to choose the size of test area;indeed, a test area too small is not representative but too large leads to lack of stability. The recommended side is a square with a length of in the range 10-30 μm. In this paper, the cement paste and the mortar were tested using the PF-QNM technique. It is shown that the PF-QNM technique is very powerful to characterize the mechanical properties of micro-and nanostructures in the cement-based materials. It does not have strict requirements for test environment and it does not damage the surface of the material. High-resolution images can be obtained very easily, and they can be analyzed statistically. The test results show that PF-QNM analysis can test not only the mechanical properties of the cement paste, but also investigate the interfacial regions in the cement-based material, including the variation in the mechanical properties of interface regions and the extension of the interfacial regions. During the test, care must be taken to choose the size of test area; indeed, a test area too small is not representative but too large leads to lack of stability. The recommended side is a square with a length of in the range 10-30 μm.
作者 REN Mei SHI Tao 任梅;施韬;David J.Corr;Surendra P.Shah(College of Management,Zhejiang University of Technology, Hangzhou 310023,China;College of Civil Engineering and Architecture,Zhejiang University of Technology,Hangzhou 310023,China;Key Laboratory of Civil Engineering Structures & Disaster Prevention and Mitigation Technology of Zhejiang Province,Hangzhou 310023,China;Department of Civil and Environmental Engineering,Northwestern University,Evanston,IL 60208,USA)
出处 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2019年第4期893-899,共7页 武汉理工大学学报(材料科学英文版)
基金 Funded by the National Natural Science Foundation of China(51778582&51879235) the National Key R&D Plan(2017YFC0804809)
关键词 PF-QNM peakforce TAPPING AFM cement PASTES mortar Young's MODULUS interface micro-and NANO-STRUCTURE NANOINDENTATION PF-QNM peakforce tapping AFM cement pastes mortar Young’s modulus interface micro-and nano-structure nanoindentation
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