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二维纳米空洞方格:诺氟沙星锰(Ⅱ)配合物(英文) 被引量：2

2D Nanoporous Molecular Square Grid:Manganese(Ⅱ) Norfloxacin Complex
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摘要 The reactions of norfloxacin(H-Norf)with Mn (ClO 4 ) 2 ·6H 2 O and Mn (OH) 2 yield Mn (H-Norf)(ClO 4 ) 2 ·2H 2 O(1)and[Mn (Norf) 2 ·4H 2 O] n (2),respectively.1is monomeric while2has a novel 2D neutral square grid with an antibacterial drug as buildi ng block.Crystal data for1:triclinic,space groupP1(No.2),a=9.0939(3),b=9.4395(3),c=12.7182(3)*!,α=111.447(2),β=90.340(2),γ=112.357(1)°,V=926.34(5)*! 3 ,Z =1,ρ cacl =1.664g·cm -3 .Mo Kαradiation(λ=0.71073*!),T=293(2)K,μ=0.595mm -1 ,R 1 =0.0692,w R 2 =0.1482for 2320observed reflectio ns from 4390independent reflection s,GOF =0.940;Crystal data for2:Monoclinic,P2 1 /c,a=5.7530(12),b=21.865(4),c=13.343(3)*!,β=98.25(3)°,V=1661.1(6)*! 3 ,Z =2,ρ cacl =1.527g·cm -3 ,T=293(2)K,μ=0.477mm -1 ,R 1 =0.0531,w R 2 =0.1552for2070observed reflections from 2870independent reflections,GOF =1.384.CCDC:140819;151063. The reactions of norfloxacin(H-Norf)with Mn (ClO 4 ) 2 ·6H 2 O and Mn (OH) 2 yield Mn (H-Norf)(ClO 4 ) 2 ·2H 2 O(1)and[Mn (Norf) 2 ·4H 2 O] n (2),respectively.1is monomeric while2has a novel 2D neutral square grid with an antibacterial drug as buildi ng block.Crystal data for1:triclinic,space groupP1(No.2),a=9.0939(3),b=9.4395(3),c=12.7182(3)*!,α=111.447(2),β=90.340(2),γ=112.357(1)°,V=926.34(5)*! 3 ,Z =1,ρ cacl =1.664g·cm -3 .Mo Kαradiation(λ=0.71073*!),T=293(2)K,μ=0.595mm -1 ,R 1 =0.0692,w R 2 =0.1482for 2320observed reflectio ns from 4390independent reflection s,GOF =0.940;Crystal data for2:Monoclinic,P2 1 /c,a=5.7530(12),b=21.865(4),c=13.343(3)*!,β=98.25(3)°,V=1661.1(6)*! 3 ,Z =2,ρ cacl =1.527g·cm -3 ,T=293(2)K,μ=0.477mm -1 ,R 1 =0.0531,w R 2 =0.1552for2070observed reflections from 2870independent reflections,GOF =1.384.CCDC:140819;151063.
作者 王立中 陈振锋 王锡森 李咏华 熊仁根 游效曾
机构地区 南京大学配位化学研究所
出处 《无机化学学报》 SCIE CAS CSCD 北大核心 2002年第12期1185-1190,共6页 Chinese Journal of Inorganic Chemistry
基金 国家重点基础研究发展规划资助项目(G2000077500) 国家自然科学基金资助项目 教育部优秀青年教师资助计划项目
关键词 纳米空洞 诺氟沙星 锰(Ⅱ)配合物 抗生素 配位化学 nanoporous norfloxacin m anganese complex
分类号 R978.1 [医药卫生—药品] R914 [医药卫生—药物化学]
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无机化学学报
2002年 第12期

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