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薇甘菊挥发油的化学成分及GC指纹图谱 被引量:2

Chemical Components and GC Fingerprint of Volatile Oil from Mikania micrantha
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摘要 采用GC-MS法分析薇甘菊挥发油化学成分,采用GC法建立其GC指纹图谱,并测定其中β-石竹烯的含量。结果表明,通过GC-MS法分析得到了薇甘菊挥发油的14个化学成分的相对含量;10批薇甘菊挥发油的GC指纹图谱显示出19个共有峰,相似度为0.80~0.95,批间相似度差异较大;以水杨酸甲酯为内标,采用GC法测定薇甘菊挥发油中β-石竹烯含量为0.00268%。该方法可为薇甘菊质量控制提供参考。 We analyzed the chemical components of the volatile oil from Mikania micrantha by GC-MS,established the GC fingerprint by GC,and determined the content ofβ-caryophyllene in the volatile oil by GC.The results show that 14 chemical components in the volatile oil from Mikania micrantha are identified by GC-MS,and their relative contents are determined.The GC fingerprints of 10 batches show 19 common peaks,the similarity is 0.80-0.95,and the similarity between batches is quite different.The content ofβ-caryophyllene in the volatile oil from Mikania micrantha is 0.00268%by GC while using methyl salicylate as an internal standard.This method can provide a reference for the quality control of Mikania micrantha.
作者 黄薏佳 朱小媚 钟碧华 宋佳堉 王术玲 HUANG Yijia;ZHU Xiaomei;ZHONG Bihua;SONG Jiayu;WANG Shuling(School of Pharmaceutical Sciences,Guangzhou University of Traditional Chinese Medicine,Guangzhou 510006,China)
出处 《化学与生物工程》 CAS 2020年第2期55-58,共4页 Chemistry & Bioengineering
基金 国家自然科学基金项目(81774193) 广东省自然科学基金项目(2017A030313716) 广州市科技计划项目(201707010443)。
关键词 薇甘菊 挥发油 化学成分 β-石竹烯 气相色谱法 指纹图谱 Mikania micrantha volatile oil chemical component β-caryophyllene gas chromatography fingerprint
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