期刊文献+

肠类制品中特布他林含量测定的不确定度研究

Study on the Uncertainty in Measuring Terbutaline in Sausage Products
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摘要 本文采用气相色谱-质谱法(GC-MS)测定肠类制品中特布他林(TBL)的残留量,同时评定了检测结果的不确定度。通过计算各个影响因素,得出测定结果的不确定度为(3.348±0.292)μg/kg,而加标回收率测定引入的不确定度是主要的不确定度因素之一。 This paper uses gas chromatography-mass spectrometry(GC-MS)to determine the TBL residues in sausage products.And the uncertainty of the results is evaluated.By calculating the influencing factors,the uncertainty of the measurement results is(3.348±0.292)μg/kg,and the uncertainty introduced by the adding recovery is one of the main uncertainty factors.
作者 耿振 姜延国 GENG Zhen;JIANG Yanguo(Dandong Health Service Centre,Liaoning Province,Dandong,Liaoning,118000,China)
出处 《检验检疫学刊》 2020年第2期44-45,共2页 Journal of Inspection and Quarantine
关键词 特布他林 不确定度 气相色谱-质谱法 Terbutaline Uncertainty GC-MS
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  • 1郭伟,杨丽君,时文春,徐成钢,崔佳,李兆杰,夏凡.高效液相色谱-串联质谱测定猪肉中3种β-受体激动剂残留量[J].分析试验室,2010,29(4):92-98. 被引量:15
  • 2孟娟,邵兵,吴国华,薛颖.气相色谱-质谱法同时测定动物性食品中8种β-兴奋剂的残留量[J].中国卫生检验杂志,2005,15(6):641-643. 被引量:37
  • 3孔莹,邱月明,李鹏,沈建忠.固相萃取/气相色谱-质谱同时测定猪肉中4种β-激动剂类药物残留量[J].分析测试学报,2006,25(2):63-66. 被引量:48
  • 4肖九长,黄承斌,吕春,林燕.45例"瘦肉精"中毒患者部分生化指标分析[J].江西医学检验,2006,24(2):186-186. 被引量:2
  • 5中华人民共和国农业部第235号公告《动物性食品中兽药最高残留限量》[s].2007.
  • 6Daniele D, Eronica M, Marco P, et al. Simultaneous de- termination of β2-agonists in uman urine by fast-gas chro- matography mass spectrometry: method validation and clinical application [J]. Biomed. Chromatogr, 2010, 24: 358-366.
  • 7Bing S, Xiao F, Jing Z, et al. Multi-residual analysis of 16 b-agonists in pig liver, kidney and muscle by ultra perform- ance liquid chromatography tandem mass spectrometry [J] . Food Chemistry, 2009, 114:1 115-1 121.
  • 8Howells L, Sauer M, Sayer R D Clark. Extraction and clean-up of the β-agonists salbutamol from liver and its determination by enzyme immuoassay [J] . Analytica Chimi- ca Acta, 1993, 275: 275-278.
  • 9Elliott T, Thompson S, Arts J, et al. Screening and con- firmatory determination of ractopamine residue in calves treated with growth promoting doses of the beta-agonist[J] . Analyst, 1998, 123:1 103-1 107.
  • 10Hing L, Kurtis S, Thomas E. Peart. Determination of β- blockers and β2-agonists in sewage by solid-phase extraction and liquid chromatography tandem mass spectrometry[J] . J Chromatogr: A, 2007, 1 148: 158- 167.

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