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HPLC-MS/MS法检测福建中部海域养殖贝类麻痹性贝类毒素 被引量:3

Detection of paralytic shellfish toxins in the farming shellfish productscollected from the middle of Fujian sea-area by high performanceliquid chromatography-tandem mass spectrometry
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摘要 实验采用高效液相色谱-串联质谱法(HPLC-MS/MS)检测2017—2018年福建中部海域养殖贝类麻痹性贝类毒素(PSTs)。结果表明:2018年采集的贝类样本均未检出麻痹性贝类毒素,2017年采集的贝类样本有17批次检出麻痹性贝类毒素,主要检出成分为脱氨甲酰基石房蛤毒素(dcSTX)、膝沟藻毒素(GTX1、GTX2、GTX3、GTX4、GTX5),脱氨甲酰基膝沟藻毒素(dcGTX2、dcGTX3)也占有一定比例,未发现石房蛤毒素(STX)。2017年福建中部海域链状裸甲藻(Gymnodinium catenatum)暴发事件对该海域养殖贝类的麻痹性贝类毒素有一定影响,其中有毒赤潮对贻贝的影响大于牡蛎,而对缢蛏和蛤类则无影响。 The paralytic shellfish toxins was investigated in farming shellfish samples collected from the middle of Fujian sea-area from the year of 2017 to 2018 by high performance liquid chromatography-tandem mass spectrometry.The results showed that:PST was not detected in the shellfish samples collected in 2018;PST was detected in the 17 batch of shellfish samples collected in 2017,with dcSTX as the most predominant components.Besides,GTX1-5 and dcGTX2-3 could also be detected in the samples.STX was not detected in the samples.The outbreak of Gymnodinium catenatum in the middle of Fujian sea-area had a certain impact on the detection of PST in the shellfish samples from the same area,including a greater impact on the mussels than oysters;but there was no impact on Sinonovacula constricta and Ruditapes philippinarum.
作者 杨云辉 YANG Yunhui(Monitoring Center of Fishery Resource of Fujian,Fuzhou 350003,China)
出处 《渔业研究》 2020年第5期473-480,共8页 Journal of Fisheries Research
基金 国家重点研发计划“战略性国际科技创新合作”重点专项项目:“一带一路”沿线国家海洋赤潮与低氧等生态灾害的发生机制与早期预警和应急保障系统的关键技术研究(2016YFE0202100).
关键词 麻痹性贝类毒素 高效液相色谱串联质谱法 链状裸甲藻 paralytic shellfish toxins(PSTs) HPLC-MS/MS Gymnodinium catenatum
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