摘要
本文深入研究了铸态AZ31-xGd(x=0,1.5 wt%,2.0 wt%,2.5 wt%)镁合金在半固态等温热处理中显微组织和富Gd相的演变。结果表明,添加Gd的AZ31镁合金中的层状(Mg,Al)3Gd相在半固态等温热处理过程中转变为颗粒状Al2Gd相,导致形成更多的球状α-Mg晶粒。当Gd含量为2.0%(质量分数)时,半固态球状晶粒的尺寸达到最小值。晶粒细化的主要机理在于树枝晶的重熔以及少量充当孕育剂的Al2Gd相的辅助作用。同时,固液界面处富集的Al2Gd颗粒可以显著阻碍α-Mg晶粒的粗化长大。与铸态AZ31镁合金(280 MPa)和半固态AZ31镁合金(209 MPa)相比,经过等温热处理的半固态AZ31-2.0Gd镁合金具有适中的压缩变形抗力(230 MPa),实现了变形阻力的降低。
The microstructure and Gd-rich phase evolution of as-cast AZ31-xGd(x=0,1.5 wt.%,2.0 wt.%and 2.5 wt.%)magnesium alloys during semi-solid isothermal heat treatment were investigated deeply in the present work.Results showed that the lamellar(Mg,Al)3Gd phases transformed into the particle-like Al2Gd phases in AZ31 magnesium alloys with Gd addition during semi-solid isothermal heat treatment,leading to yielding more sphericalα-Mg grains.When Gd content is 2.0 wt.%,the size of semi-solid spherical grains reaches the minimum.The main mechanism of grain refinement lies in the remelting of dendritic branches as well as the auxiliary effect of a small number of Al2Gd particles as grain refining inoculants.Meanwhile,Al2Gd particles enriched at the solid-liquid interfaces can remarkably retard the growth rate ofα-Mg grains.A reduction of deformation resistance has been successfully achieved in AZ31-2.0Gd magnesium alloy after semi-solid isothermal heat treatment,which shows a moderate compressive deformation resistance(230 MPa),comparing to the as-cast AZ31 magnesium alloy(280 MPa)and semi-solid AZ31 magnesium alloy(209 MPa).
作者
褚晨亮
吴孝泉
邱水才
汤斌兵
殷正
闫洪
罗超
胡志
CHU Chen-liang;WU Xiao-quan;QIU Shui-cai;TANG Bin-bing;YIN Zheng;YAN Hong;LUO Chao;HU Zhi(Institute of Advanced Forming,Nanchang University,Nanchang 330031,China;Changzhou University Huaide College,Jingjiang 214513,China;Institute for Advanced Study,Nanchang University,Nanchang 330031,China)
基金
Project(20171BAB206005)supported by the Natural Science Foundation of Jiangxi Province,China
Project(20153BCB23023)supported by the Training Program Foundation for Young Scientists of Jiangxi Province,China
Project(51961026)supported by the National Natural Science Foundation of China。
关键词
镁
显微组织
稀土元素
Al2Gd颗粒
半固态等温热处理
magnesium
microstructure
rare earth element
Al2Gd particle
semi-solid isothermal heat treatment