摘要
本文采用气相色谱法,使用Agilent DB-1701毛细管色谱柱对N-(2-氯乙基)甲磺酰胺进行定性分析,以苯甲酸丁酯为内标物进行定量分析。该分析方法峰形尖锐对称,分析速度快,标准偏差为0.08,变异系数为0.09%,回收率为99.00%~101.00%之间。
The qualitative analysis of N-(2-chloroethyl) methanesulfonamide was carried out on Agilent DB-1701 capillary column by gas chromatography with butyl benzoate as internal standard.The method has sharp and symmetrical peak shapeand fast analysis speed.The standard deviation,coefficient of variationand recovery were 0.08,0.09% and 99.00%~101.00%respectively.
作者
刘红翼
LIU Hong-yi(Shenyang Research Institute of Chemical Industry Co.,Ltd.,Shenyang 110021,Liaoning China)
出处
《染料与染色》
CAS
2020年第6期46-48,共3页
Dyestuffs and Coloration
关键词
N-(2-氯乙基)甲磺酰胺
气相色谱
内标定量分析方法
N-(2-Chloroethyl)methanesulfonamide
gas chromatography
method of internal standard quantity analysis
