摘要
建立了测定橘皮精油中d-柠檬烯的高效液相色谱方法。实验结果表明该方法具有操作简便、快速、准确、分离效果好的特点,准确度和精确度均能满足定量分析的要求。
A HPLC method for the determination of D-limonene in orange peel essential oil was established. The method adopts a stainless steel column and diode array detector with ODS-2 C18 5 m as packing. Using methanol/acetonitrile/water = 63/22/15 as mobile phase,96% D-limonene in orange peel essential oil was isolated and quantitatively detected at 205 nm wavelength.The results showed that the linear correlation coefficients of were 0. 9999,standard deviations were 0. 015,variation coefficients were 0. 14%;the average recoveries were 99. 99%.
作者
蓝宏彦
吴燕飞
何玉清
Lan Hongyan;Wu Yianfei;He Yuqing(Liuzhou Huinong Chemical Company,Liuzhou 545616,China)
出处
《山东化工》
CAS
2020年第24期94-96,共3页
Shandong Chemical Industry
