期刊文献+

环状硝酮中间体己醛肟的合成方法研究

下载PDF
导出
摘要 在目前已有的环状硝酮的合成路线的基础上,对3,4-双-苄氧基-2-(1,2-双-苄氧基-乙基)-5-甲氧基-四氢-呋喃(甲苷)的水解和2,3,5,6-四-苄氧基-4-碘-氧-叔丁基二甲硅基-己醛肟的合成这两步进行更多反应条件的尝试,改变了这两步反应所用的催化剂和pH值,并对己醛肟的形成使用了微波辐射和超声辐射催化法进行了探索。
出处 《石油石化物资采购》 2021年第6期36-37,共2页 Petroleum & Petrochemical Material Procurement
基金 华北理工大学大学生创新创业训练计划项目(X2018324).
  • 相关文献

参考文献2

二级参考文献12

  • 1Shibano M,Tsukamoto D,Masuda A,et al.Two new pyrrolidine alkaloids,radicamines A and B,as inhibitors of α-glucosidase from lobelia chinensis LOUR[J].Chem Pharm Bull,2001,49(10):1362-1365.
  • 2Liu C Y,Gao J C,Yang G,et al.Enantiospecific synthesis of (-)-radicamine B[J].Lett Org Chem,2007,4(12):556-558.
  • 3Yu C Y,Huang M H.Radicamines A and B:Synthesis and revision of the absolute configuration[J].Org Lett,2006,8(14):3021-3024.
  • 4Gurjar M K,Borhade R G,Puranik,V G,et al.Total synthesis of (-)-radicamine B[J].Tetrahedron Lett,2006,47(39):6979-6981.
  • 5Tsou E L,Chen S Y,Yang M H,et al.Synthesis and biological evaluation of a 2-aryl polyhydroxylated pyrrolidine alkaloid-based library[J].Bioorg Med Chem,2008,16(24):10198-10204.
  • 6Barker R,Fletcher H G.2,3,5-Tri-O-benzyl-D-ribosyl and -L-arabinosyl bromides[J].J Org Chem,1961,26(11):4605-4609.
  • 7Tejima S,Fletcher H G.Syntheses with partially ben zylated sugars.Ⅱ.1 The anomeric 1-O-benzoyl-L-arabinopyranoses and 1-O-benzoyl-L-arabinofuranoses and their tendencies to undergo acyl migration[J].J Org Chem,1963,28(11):2999-3004.
  • 8Bernet B,Mangholz S E,Briner K,et al.Glycosylidene diaziridines:Stereoselective addition of ammonia and methylamine to lactone oxime sulfonates[J].Helv Chim Acta,2003,86(5):1488-1521.
  • 9Carmona A T,Robina I,Wightman R H,et al.Synthesis and glycosidase inhibitory activity of 7-deoxycasuarine[J].Helv Chim Acta,2003,86:3066.
  • 10Merino P,Revuelta J,Tejero T,et al.Fully stereoselective nucleophilic addition to a novel chiral pyrroline N-oxide:Total syntheses of (2S,3R)-3-hydroxy-3-methylproline and its (2R)-epimer[J].Eur J Org Chem,2004:776-782.

共引文献5

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部