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气相色谱质谱法测定固定污染源废气中挥发性有机物 被引量:2

Determination of VOCs in Waste Gas from Stationary Pollution Sources by GC-MS
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摘要 VOCs不仅本身具有较强毒性,还是影响中国区域大气污染的重要前兆和参与者,国内已有一些检测VOCs的现行标准,但由于现实检测情况比较复杂,很难严格按照标准方法执行。本实验通过优化P&T参数和GC-MS的条件,建立了一种准确测定固定污染源废气中VOCs的方法。该方法的线性相关拟合度较高,所测物质线性相关系数均在0.9970以上,相关化合物的检出限为0.001-0.027mg/m^(3),相对标准偏差(RSD)<7.98%,可满足相关标准的要求。 VOCs not only have strong toxicity,but are also important precursors and participants that affect the regional air pollution in my country.There are some existing standards for testing VOCs in China,but due to the complicated actual testing situation,it is difficult to strictly follow the standard methods..This experiment established a method for accurately determining VOCs in exhaust gas from stationary sources by optimizing P&T parameters and GC-MS conditions.The method has a high degree of linear correlation fitting.The linear correlation coefficients of the tested substances are all above 0.9970,the detection limit of related compounds is 0.001-0.027 mg/m^(3),and RSD is<7.98%,which can meet the requirements of relevant standards.
作者 叶继 Ye Ji(Maoming Environmental Protection Monitoring Station,Maoming 525000,China)
出处 《粘接》 CAS 2021年第8期50-53,共4页 Adhesion
关键词 气相色谱质谱法 吹扫捕集 固定污染源 VOCs排放 GC-MS P&T stationary pollution sources VOCs emissions
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  • 1陈国征,王炫征,钱洪智,蒋斌.正已烷萃取气相色谱法测定水中苯系物[J].中国卫生检验杂志,2006,16(4):491-492. 被引量:10
  • 2陆思华,白郁华,张广山,李湉湉.大气中挥发性有机化合物(VOCs)的人为来源研究[J].环境科学学报,2006,26(5):757-763. 被引量:127
  • 3Bianchi AP, Varney MS.. Sampling and analysis of VOCs in estuarine air by GS-MS J. of Chrom[J],1993,643: 11-23.
  • 4Wolkoff P, Wilkins CK , Clausen PA . Larsen K:Comparison of VOCs from processed paper and.toners from office and printers: Method , emission rates and modeled concentrations Indoor Air [J],1993,3:113-123.
  • 5Perkin Elmer GCBU , TECHNICAL ASSISTANCE DOCUMENT FOR US EPA METHOD TO-17[R],1996, 1-74.
  • 6Wejnerowska G, Gaca J. Application of headspace solid- phase microextraction for determination of chloroorganiccompounds in sewage samples [ J ]. Toxicology Mechanisms and Methods, 2008, 18 : 543 - 550.
  • 7国家环境保护总局,国家质量监督检验检疫总局.GB3838,地表水环境质量标准[S].北京:中国环境科学出版社,2002.
  • 8Kubinec R, Adamuscin J, Jurdakova H, Foltin M, Ostrovsky I, Kraus A, Sojak L. Gas chromatographic determination of benzene, toluene, ethylbenzene and xylenes using flame ionization detector in water samples with direct aqueous injection up to 250p.L [ J]. Journal of Chromatography A, 2005, 1084( 1 ) : 90 - 94.
  • 9Aeppli C, Berg M, Hofstetter T B, Kipfer R, Schwar- zenbach R P. Simultaneous quantification of polar and non-polar volatile organic compounds in water samples by direct aqueous injection-gas chromatography/mass spectrometry [ J ]. Journal of Chromatography A, 2008, 1181(1 -2) : 116 -124.
  • 10中国国家标准化管理委员会.GB/T5750.8,生活饮用水卫生标准;有机物指标[S].北京:中国标准出版社,2006:36-39.

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