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竹叶花椒挥发油析出物的波谱分析 被引量:4

Spectroscopic Analysis of the Precipitate from the Essential Oil of Zanthoxylum armatum DC
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摘要 探究竹叶花椒挥发油的成分及其变化。以竹叶花椒为原料,采用水蒸气蒸馏法获得挥发油,冷却得到挥发油析出物,利用红外光谱、核磁共振波谱和气相色谱-质谱联用仪对挥发油析出物及素油进行谱学分析。竹叶花椒挥发油素油中共分离鉴定出49种化合物,主要有烯烃类、醇类、醛酮类、酯类物质等;晶体中共分离鉴定出36种,主要含芳樟醇和醛类物质。将竹叶花椒挥发油冷却,容易获得主要成分为芳樟醇的晶体析出物。 To explore the components and variety of the essential oil from Zanthoxylum armatum DC, the essential oil was obtained by steam distillation, and the precipitate of essential oil was obtained by cooling. Spectroscopic analysis of decrystallized oil and crystal from the essential oil of Zanthoxylum armatum DC was tested by infrared spectroscopy, nuclear magnetic resonance spectroscopy and gas chromatography-mass spectrometry. A total of 49 compounds were isolated and identified of the de-crystallized oil, mainly including alkenes, alcohols, aldehydes ketones, esters and so on;A total of 36 compounds were isolated and identified in the crystal precipitate, mainly containing linalool and aldehydes. The crystal precipitate with linalool as the main component could be easily obtained by cooling the volatile oil of Zanthoxylum armatum DC.
作者 周孟焦 何鑫柱 陈凯 康明 梁晓峰 ZHOU Mengjiao;HE Xinzhu;CHEN Kai;KANG Ming;LIANG Xiaofeng(School of Materials and Engineering,Southwest University of Science and Technology,Mianyang 621010;Laboratory of Research Development and Utilization on Traditional Chinese Medicine Resources in Northwest Sichuan,Sichuan College of Traditional Chinese Medicine,Mianyang 621010)
出处 《食品工业》 CAS 2021年第11期340-343,共4页 The Food Industry
基金 四川省中医药管理局科学技术研究专项课题,编号:2020JC0120 绵阳市科技项目,编号:2020YFZJ004 四川中医药高等专科学校科研项目(19BSZR01)。
关键词 竹叶花椒 挥发油 素油 晶体 成分分析 Zanthoxylum armatum DC essential oil de-crystallized oil crystal component analysis
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