摘要
目的建立瑶药材犁头草的质量标准。方法从性状、显微、薄层色谱(TLC)方面对12个批次犁头草进行定性鉴别,按照药典方法测定药材水分、总灰分及酸不溶性灰分、浸出物。结果各鉴别方法专属性强,12批犁头草药材色谱与对照品色谱在相同位置,显相同颜色的荧光斑点;药材水分为8.72%~11.61%,总灰分为10.03%~18.31%,酸不溶性灰分为1.17%~5.91%,纯水浸出物含量为29.06%~37.16%。结论该研究建立的质量标准可用于瑶药材犁头草的质量评价。
Objective To establish the quality standard of Yao medicine Violae inconspicuae herba.Methods Twelve batches of Vi⁃ola inconspicua Blume were identified in respects of properties,microscopic characteristics and TLC.According to the Pharmacopoeia method,moisture,total ash,acid insoluble ash and extractives were determined.Results Identification methods were highly specific.The chromatogram of 12 batches of Viola inconspicua Blume.presented the fluorescence spots of the same colors as the control at the corresponding position.The contents of moisture,total ash,acid-insoluble ash,water-soluble extract were 8.72%-11.61%,10.03%-18.31%,1.17%-5.91%,and 29.06%-37.16%,respectively.Conclusion The established standard can be used for quality evaluation of Yao medicine Violae inconspicuae herba.
作者
何瑞婷
朱华
黎理
张淼
谢凤凤
黄飘玲
杨雯琪
董雪静
HE Ruiting;ZHU Hua;LI Li;ZHANG Miao;XIE Fengfeng;HUANG Piaoling;YANG Wenqi;DONG Xuejing(Guangxi University of Chinese Medicine,Guangxi Key Laboratory of Zhuang and Yao Ethnic Medicine,Nanning,Guangxi Zhuang Autonomous Region 530200,China)
出处
《安徽医药》
CAS
2022年第2期221-224,共4页
Anhui Medical and Pharmaceutical Journal
基金
国家自然科学基金资助项目(81260620、81460587)
广西壮瑶药重点实验室(桂科基字〔2014〕32号)
壮瑶药协同创新中心(桂教科研〔2013〕20号)
广西一流学科中药学(民族药学)(桂教科研〔2018〕12号)
广西重点学科(壮药学)(桂教科研〔2013〕16号)
第八批广西壮族自治区特聘专家项目(桂人才通字〔2019〕13号)
第一批“港澳台英才”入桂计划项目(桂科智字〔2019〕42号)
广食品药品监督管理局瑶药材质量标准第二卷(YJJ17007、YJJ17008、YJJ17014)
广西中医药大学硕士研究生科研创新项目(YCSY20190038)。
关键词
堇菜属
医学
传统
瑶药材
犁头草
显微鉴别
薄层鉴别
质量标准
瑶族
Viola
Medicine,traditional
Yao medicine
Violae inconspicuae herba
Microscopic identification
TLC
Quali⁃ty standard
Yao zu