摘要
The superplasticity of Ti-43Al-9V-0.2Y alloy sheet hot-rolled at 1100℃was systematically investigated in the temperature range of 750-900℃under an initial strain rate of 10^(-4)s^(-1).A bimodalγgraindistribution microstructure of Ti Al alloy sheet,with abundant nano-scale or sub-micronγlaths embedded insideβmatrix,exhibits an impressive superplastic behaviour.This inhomogeneous microstructure shows low-temperature superplasticity with a strain-rate sensitivity exponent of m=0.27 at 800℃,which is the lowest temperature of superplastic deformation for Ti Al alloys attained so far.The maximum elongation reaches~360%at 900℃with an initial strain rate of 2.0×10^(-4)s^(-1).To elucidate the softening mechanism of the disorderedβphase during superplastic deformation,the changes of phase composition were investigated up to 1000℃using in situ high-temperature X-ray diffraction(XRD)in this study.The results indicate thatβphase does not undergo the transformation from an ordered L2;structure to a disordered A2 structure and cannot coordinate superplastic deformation as a lubricant.Based on the microstructural evolution and occurrence of bothγandβdynamic recrystallization(DR)after tensile tests as characterized with electron backscatter diffraction(EBSD),the superplastic deformation mechanism can be explained by the combination of DR and grain boundary slipping(GBS).In the early stage of superplastic deformation,DR is an important coordination mechanism as associated with the reduced cavitation and dislocation density with increasing tensile temperature.Sufficient DR can relieve stress concentration arising from dislocation piling-up at grain boundaries through the fragmentation from the original coarse structures into the fine equiaxed ones due to recrystallization,which further effectively suppresses apparent grain growth during superplastic deformation.At the late stage of superplastic deformation,these equiaxed grains make GBS prevalent,which can effectively avoid intergranular cracking and is conducive to the further improvement in elongation.This study advances the understanding of the superplastic deformation mechanism of intermetallic Ti Al alloy.
基金
the financial support from the Singapore Ministry of Education Academic Research Funds(R-265–000–686–114 and MOE2018-T2–1–140)。
