摘要
As a family of two-dimensional functional materials, layered double hydroxides(LDHs) have the characteristics of adjustable lamellar element type and proportion, variable interlamellar anion, controllable particle size and thickness, providing a robust platform for photo/electro/thermal-catalysis. With the continuous progress of materials science, the synthesis of LDHs is becoming more and more refined. Herein, to achieve the fine preparation of LDHs materials, especailly for the no-chemical/material researchers, we successfully assembled the automatic synthesis device and wrote corresponding computer software to control this device, and the automatic synthesis of bulk and monolayer LDHs nanosheets on a laboratory scale can be realized. This work paves a new labor-saving way for the fine synthesis of LDHs nanostructures, further improving the development of LDHs-based materials.
基金
This work was supported by the National Natural Science Foundation of China(Nos.21922801,21878008)
the Beijing Natural Science Foundation,China(Nos.2202036,2182047)
The XAFS experiments were conducted in 1W1B beamline of the Beijing Synchrotron Radiation Facility(BSRF),China.
