浅谈气相色谱法检测果蔬中农药残留能力验证操作技巧及关键被引量：4

原文传递

导出

摘要本文阐述了果蔬中有机磷、有机氯、拟除虫菊酯类农药残留能力验证盲样考核气相色谱法检测的方法、步骤,以及易出现问题的关键环节和应对的措施。

作者俞晓

机构地区乌鲁木齐市农产品质量安全检测中心

出处《新疆农业科技》 2022年第3期17-18,共2页 Xinjiang Agricultural Science and Technology

关键词气相色谱法农残能力验证技巧关键

分类号 S481.8 [农业科学—农药学] O657.71 [理学—分析化学]

引文网络
相关文献

参考文献6

1张登洲,李小燕,张钰杰,李洁笠.气相色谱法测定蔬菜水果中农药残留能力验证标准化初探[J].食品安全导刊,2020(33):118-119. 被引量：4
2田强.农产品中农药残留检测能力验证存在的问题以及关键点控制[J].食品安全导刊,2021(26):43-44. 被引量：6
3王璐,刘潇威,彭祎,罗铭.我国农产品质量安全检测机构农药残留检测能力验证现状分析[J].农业环境与发展,2012,29(3):90-92. 被引量：17
4帅云,万宏伟,王娟,覃事玉.农产品质量安全检测机构农药残留检测能力验证的方法与技巧[J].现代食品,2018,3(22):84-87. 被引量：10
5田雪莲,兰承兴,周开拓,李雪林.农产品农药残留检测能力验证的影响因素及对策[J].农技服务,2020,37(12):87-87. 被引量：5
6黄宝勇,欧阳喜辉,潘灿平.色谱法测定农产品中农药残留时的基质效应[J].农药学学报,2005,7(4):299-305. 被引量：97

二级参考文献52

1NY 1500.13.3-41500.31.1-49.2-2008.蔬菜、水果中甲胺磷等20种农药最大残留限量[S].
2GB 2763-2005,食品中农药最大残留限量[S].
3Zrostlfkova J, Hajslova J, Godula M, et al. Performance of programmed temperature vaporizer, pulsed splitless and on-column injection techniques in analysis of pesticide residues in plant matrices[J]. J Chromatogr A, 2001, 937: 73-86.
4Fernandez-Gonzalez C, Rial-Otero R, Cancho-Grande B, et al.Determination of fungicide residues in white grapes for winemaking by gas chromatography with mass spectrometric detection and assessment of matrix effects [J]. J AOAC Int,2003, 86: 1008-1014.
5Albero B, Sanchez-Brunete C, Tadeo J L. Analysis of pesticides in honey by solid-phase extraction and gas chromatography-mass spectrometry[J]. J Agric Food Chem, 2004, 52: 5828-5835.
6Anastassiades M, Mastovska K, Lehotay S J. Evaluation of analyte protectants to improve gas chromatographic analysis of pesticides[ J]. J Chromatogr A, 2003, 1015 : 163-184.
7Gonzalez-Egea F J, Hemandez-Torres M E, Almansa-Lapez E,et al. Matrix-effects of vegetable commodities in electron-capture detection applied to pesticide multiresidue analysis [J]. J Chromatogr A, 2002, 966 : 155-165.
8Cuadms-Rodriguez L, Garcia-Campana A M, Almansa-Lopez E,et al. Correction function on biased results due to matrix effects application to the routine analysis of pesticide residues [ J ].Analytica Chimica Acta, 2003, 478: 281-301.
9Martinez-Galem M, Lopez-Lopez T, Gil-Garcia M D, et al. A comparative study of the correction of systematic errors in the quantitation of pyrethroids in vegetables using calibration curves prepared using standards in pure solvent [ J ]. Anal Bioanal Chem, 2003, 375 : 653-660.
10Benijts T, Dams R, Lambert W. Countering matrix effects in environmental liquid chromatography-electrospmy ionization tandem mass spectrometry water analysis for endocrine disrupting chemicals[J]. J Chromatogr A, 2004, 1029: 153-159.