期刊文献+

固相微萃取-气相色谱-质谱在《江友渚等七挖书画轴》挥发性有机化合物分析中的应用 被引量:2

Application of solid phase microextraction and gas chromatography-mass spectrometry to the volatile organic compound analysis of a scroll painting
下载PDF
导出
摘要 文化遗产的气味不仅反映了文物的历史信息,还对文化遗产自身产生持续性的影响,因此了解文化遗产的气味对其价值研究和当代保护都具有重要意义。本工作采用固相微萃取-气相色谱-质谱技术对中国国家博物馆藏《江友渚等七挖书画轴》天头用纸散发的气体进行了采集、分离和分析。结果表明:与纸张降解相关的标志物(如脂肪酸、醛、酮等)得到有效采集;而其他生物标记物(如沉香螺醇)的检出也反映了该书画轴的历史保存环境信息。此方法对该件书画轴的历史价值认知和科学保护具有重要作用。 The odors of cultural heritage objects not only reflect their historical information,but also have lasting impacts on the objects themselves.Therefore,understanding the odors of cultural heritage objects is of great significance for research and contemporary conservation.In this work,solid phase microextraction(SPME)and gas chromatography-mass spectrometry(GC-MS)were used to collect,separate and analyze the odors emitted from the head margin paper of a scroll painting collected in the National Museum of China.The results show that the method could effectively collect markers related to paper degradation(such as fatty acids,aldehydes and ketones).In addition,the detection of other biomarkers(such as agarospirol)also reflects information about the historical preservation environments of the scroll.This method plays an important role in understanding the historical value and scientific conservation of the painting.
作者 丁莉 杨琴 李郑 DING Li;YANG Qin;LI Zheng(National Museum of China,Beijing 100006,China)
机构地区 中国国家博物馆
出处 《文物保护与考古科学》 北大核心 2022年第4期105-113,共9页 Sciences of Conservation and Archaeology
基金 中国国家博物馆馆级课题(GBKX2019Y01)资助。
关键词 固相微萃取-气相色谱-质谱 挥发性有机化合物 中国书画 SPME-GC-MS VOC Chinese painting and calligraphy
  • 相关文献

参考文献5

二级参考文献24

  • 1杨友宝,宁德山.中药沉香挥发油成分分析[J].湖南中医杂志,2004,20(5):48-49. 被引量:16
  • 2刘军民,徐鸿华.国产沉香研究进展[J].中药材,2005,28(7):627-632. 被引量:77
  • 3彭强.七批沉香的检验[J].中药材,1989,12(2):21-24. 被引量:1
  • 4梁振益,张德拉,刘长生,杨劲锋.CGC-MS法测定白木香挥发油的化学成分[J].海南大学学报(自然科学版),2005,23(3):228-232. 被引量:14
  • 5宋振玉.中草药现代研究(第三卷)[M].北京医科大学和中国协和医科大学联合出版社,1997,8.413-420.
  • 6Okugawa H,Ueda R,Matsumoto K,et al.Effect of jinkoh-eremol and agarospirol from agarwood on the central nervous system in mice.Planta Med,1996,62(1):2-6.
  • 7Kanako Satoh,Fumiko Nagai,Itsu Kano.Inhibition of H^+,K^+ -ATPase by hinesol,a major component of So-jutsu,by interaction with enzyme in the E1 state.Biochemical Pharmacology,2000,59 (7):881-886.
  • 8Yamahara J,Li Y H,Tamai Y.Anti-ulcer effect in rats of bitter cardamon constituents.Chem Pharm Bull,1990,38:3053-4.
  • 9Hendriks H,Bos R,Woerdenbag H J.Central nervous depressant activity of valerenic acid in the mouse.Plants Med.,1985,49(1):28-31.
  • 10Okugawa H,Ueda R,Matsumoto K,et al.Effects of sesquiterpenoids from "Oriental incenses" on acetic acid-induced writhing and D2 and 5-HT2A receptors in rat brain.Phytomedicine,2000,7 (5):417-422.

共引文献135

同被引文献46

引证文献2

二级引证文献2

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部