Continuous observation of twinning and dynamic recrystallization in ZM21 magnesium alloy tubes during locally heated dieless drawing

Compared to cold drawing,dieless drawing has shown great potential for manufacturing biodegradable Mg alloy microtubes due to the large reduction in area acquired in a single pass.However,owing to the local heating and local deformation,the deformation mechanism during dieless drawing is not clear,and thus causing difficulties in controlling the microstructure of dieless drawn tubes.For the purpose of acquiring a desired microstructure.in this study the deformation mechanism of ZM21 Mg alloy tube was clarified by conducting continuous observation of the microstructural evolution during dieless drawing.The results show that both SRX and DRX occurred during dieless drawing.SRX occurred before the plastic deformation to soften dieless drawn tubes.With increase of feeding speed,the deformation mechanism changed accordingly:(1) At the low-speed of 0.02 mm/s,the deformation mechanism was dominated by twin-slip sliding,during which {10-12} tension twins were generated inside grains to accommodate the plastic deformation by changing the crystal orientation.(2) At the intermediate-speed of 2 mm/s,a twin-DRX process related to {10-12} tension twin was observed,which was characterized by the generation of abundant {10-12} tension twins and the evolution of misorientation angle of {10-12} tension twins.Moreover,the transformation from twin-DRX to CDRX can be observed at the late stage of plastic deformation,which was attributed to the inhomogeneous conditions of dieless drawing.(3) At the high-speed of 5 mm/s,a CDRX process was observed,during which grain boundary sliding and grain tilting were observed,in addition to the gradual rotation of subgrains.These results show that during dieless drawing,DRX is not only a temperature-dependent phenomenon,but also influenced by the variation of feeding speed.