摘要
应用气相色谱法,测定盐酸羟胺中甲酸的含量。为了确保方法的准确性和可行性,进行了方法学验证性实验:测定方法专属性、线性试验、检测限和定量限、精密度和回收率。结果表明:该方法对于测定盐酸羟胺中甲酸具有可行性。
In order to accurately determine the content of formic acid in hydroxylamine hydrochloride,gas chromatography was used to determine the content of formic acid in hydroxylamine hydrochloride under certain chromatographic conditions.At the same time,in order to ensure the accuracy and feasibility of the method,we carried out methodological validation experiments through determination of specificity,linearity test,detection limit and quantification limit,precision and recovery rate.The experimental results show that this method is feasible for the determination of formic acid in hydroxylamine hydrochloride.
作者
郑滔
陈鹏
汪华
王涛
刘晓宇
钟旭斌
Zheng Tao;Chen Peng;Wang Hua;Wang Tao;Liu Xiaoyu;Zhong Xubin(Livzon Syntpharm Co.,Ltd.(Zhuhai FTZ),Zhuhai 519030,China;Institute of Teacher Education,Taishan University,Tai'an 271021,China)
出处
《云南化工》
CAS
2023年第4期61-63,共3页
Yunnan Chemical Technology
关键词
盐酸羟胺
甲酸
气相色谱法
hydroxylamine hydrochloride
formic acid
feasible