3-甲基吡啶的合成工艺研究

Study on the Synthetic Process of 3-Methylpyridine

简要介绍了3-甲基吡啶的用途和微波液相的合成方法。实验考查并优化了碳源种类、氨源种类、催化剂用量、不同溶剂、反应时间等一系列条件,最终3-甲基吡啶的选择性和收率分别达到65%和71.2%。

The application of 3-methylpyridine and the synthesis method of microwave liquid phase were briefly intro⁃duced.Different carbon sources,ammonia sources,catalyst dosages,different solvents and reaction time were explored.A series of conditions such as carbon source type,ammonia source type,catalyst dosage,different solvents and reaction time were investigated and optimized in the experiment.Finally,the selectivity and yield of 3-methylpyridine reached 65%and 71.2%.