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基于氮掺杂硅量子点检测Cr(Ⅵ)的荧光传感新方法

A new fluorescence sensing method for Cr(Ⅵ)detection based on nitrogen-doped silicon quantum dots
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摘要 建立了一种用于环境水样和食物样品中Cr(Ⅵ)含量检测的新方法。该方法以氮掺杂硅量子点(N-SiQDs)作为荧光探针,在λex=360 nm条件下,荧光强度随着Cr(Ⅵ)浓度的变化呈线性猝灭关系。线性范围分别为0.5~5.0μg mL^(-1)和5.0~12.0μg mL^(-1),检出限为0.16μg mL^(-1),RSD=0.56%,并成功用于环境水样和食物样品中Cr(Ⅵ)的检测。该方法具有操作简单、灵敏度高、速度快、成本低廉等优点。 This study develops a new method for the determination of Cr(VI)in environmental water samples and food samples,which uses nitrogen-doped silicon quantum dots(N-SiQDs)as fluorescent probes.It finds that the fluorescence intensity of N-SiQDs presents a good linear relationship with the concentration of Cr(VI)atλex=360 nm.And the linear ranges are 0.5~5.0μg mL^(-1) and 5.0~12.0μg mL^(-1),with the detection limits of 0.16μg mL^(-1) and RSD=0.56%.This developed method has also been successfully used for the detection of Cr(VI)in different matrix samples.It is efficient,easy to operation,low in cost and has high sensitivity.
作者 吴一微 董淼 曹杰 WU Yi-wei;DONG Miao;CAO Jie(Hubei Collaborative Innovation Center for Rare Metal Chemistry,Hubei Key Laboratory of Pouutant Analysis and Reuse Technology,Huangshi 435002,China;College of Chemistry and Chemical Engineering,Hubei Normal University,Huangshi 435002,China)
出处 《湖北师范大学学报(自然科学版)》 2023年第4期33-38,共6页 Journal of Hubei Normal University:Natural Science
关键词 硅量子点 荧光探针 Cr(Ⅵ) Silicon quantum dots Fluorescent probe Cr(VI)
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