摘要
根据钼精矿制备二硫化钼的生产特点和存在问题,设计了一套高剪切外循环反应装置用于酸浸法制备二硫化钼的工艺,利用高剪切均质泵特有的乳化、剪切、摩擦、撞击功能,将固体颗粒细化并表面不断更新,强化反应过程,缩短反应时间,提高产品品质。外循环通过加装列管换热器增加了反应体系的换热面积,增强系统的传热效果,提高生产效率。
According to the production characteristics and existing problems of preparing molybdenum disulfide from molybdenum concentrate,a set of high shear external circulation reactor was designed for the preparation of molybdenum disulfide by acid leaching.The solid particles were refined and the surface was renewed continuously by the emulsification,shearing,friction and impact functions of high shear homogeneous pump,and the reaction process was strengthened.The reaction time is short and the product quality is improved.External circulation through the installation of tube heat exchanger increased the heat transfer area of the system and enhanced the heat transfer effect of the system so as to improve the production efficiency.
作者
成兰兴
赵增兵
张圆春
丁为公
张碧波
成馨荷
Cheng Lanxing;Zhao Zengbing;Zhang Yuanchun;Ding Weigong;Zhang Bibo;Cheng Xinhe(Henan Province Chemical Industry Research Institute Company Limited,Zhengzhou,Henan 450052,China; Luoyang Shenyu Molybdenum Industry Company Limited,Luoyang,Henan 471000,China;College of information and business,Zhongyuan University of Technology,Zhengzhou,Henan 450000,China)
出处
《化学世界》
CAS
CSCD
2019年第1期60-64,共5页
Chemical World
基金
河南省科技计划(No.182102210344)
河南省科学院助推科技成果转化专项(No.18ZT08005)资助项目
关键词
高剪切外循环
反应装置
二硫化钼
应用
high shear external circulation
reaction device
molybdenum disulfide
application