摘要
本文应用Finnigan Mat 1020 GC/MS仪,以SE-54熔融硅毛细柱作分离柱,建立了尸体脏器中敌百虫及其主要代谢物DDVP和水合氯醛的分析方法。样品用CH_2Cl_2提取。敌百虫和DDVP的检测限均是15 ng,方法已成功用于刑事案件鉴定。
Finnigan Mat 1020 GC/MS instrument and SE-54-fused silicon capillary column were adoptedto develop method for determining trichlorfon and its major metabolites, DDVP and chloralhy.drate, in corpse tissues. The detection limit of trichlorfon and its metabolites are 15ng, This me-thod has been successfully used in criminal cases.
关键词
敌百虫
DDVP
尸体脏器
毛细柱GC/MS
Trichlorfon
Chloralhydrate
DDVP
Capillary column GC/MS
Postmortem tissues
