新型溶胶-凝胶富勒烯固相微萃取涂层的研制及性能评价
被引量:1
摘要
首次采用溶胶-凝胶技术制备了新型溶胶-凝胶富勒烯固相微萃取涂层,并用扫描电镜考察其表面结构,用气相色谱法研究了它的热稳定性,耐溶剂冲洗能力。探讨了它对多氯联苯的构型选择性以及对多环芳烃,酞酸酯等的萃取能力。尝试对极性物质芳香胺进行分析。
同被引文献49
-
1吴晓苹,陈小燕,郑敏敏.毛细管电泳-安培检测法分离分析手性药物索他洛尔[J].分析化学,2010,38(12):1776-1780. 被引量:7
-
2Kraly J,Fazal M A,Schoenherr R M,etal.Bioanalytical ap-plications of capillary electrophoresi[J].Analytical Chemis-try,2006,78(12):4097-4110.
-
3Lauer H H,McManigill D.Mobile-phase transport properties of liquefied gases in near critical and supercritical fluid chroma-tography [J].Analytical Chemistry,1983,55(8):1370-1375.
-
4Cao F,Zhu X,Luo Z,et al.A novel cationic triblock copoly-met asnoncovalent coating for the separationo proteins by CE [J].Electrophoresis,2011,32(20):2874-2883.
-
5Song L G,Zhang S M,Ou Q Y,et al.Studies of crude ehlo-roformextract o roots of podophyllum-emoddii varchinesis sprague by micellar electrokinetic chromatography[J].Chrom-atographia,1994,39(11-12):682-686.
-
6Schwer C,Kenndler E,Electrophoresis in fused-silica capillar-ies:the influence of organic solvents on the electroosmotic ve-locity and the.zeta.potential [J].Analytical Chemistry,1991,63(17):1801-1807.
-
7Znaleziona J,Pelt J,Maier V,et al.Capillary electrophoresis as a verification tool for immunochemical drug screening[J].Biomed Pap Med Fac Univ Palacky Olomouc Czech Repub,2007,151(1):31-36.
-
8O"Mahony T,Owens V P,Murrihy J P,et al.Alkylthiol gold nanoparticles in opentubular capillary electroehromatog-raphy[J].Journal of Chromatography A,2003,1004(1-2):181-193.
-
9Hamer M,Yone A,Rezzano I.Gold nanoparticle-coated cap-illaries for protein and peptide analysis on opentubular capil-lary electrochromatography [J].Electrophoresis,2012,33(2):334-339.
-
10Yang L,Guihen E,Holmes J D,et al.Gold nanoparticle-modified etched capillaries for open-tubular capillary electro-chrornatography[J].Analytical Chemistry,2005,6(77):1840-1846.
-
1张伟亚,杨左军,王成云,谢丽琪,蓝芳,潘坤永,吴采樱.新型固相微萃取测定聚氯乙烯玩具制品在模拟人体汗液中的邻苯二甲酸酯增塑剂溶出量[J].化学世界,2003,44(10):520-523. 被引量:13
-
2温祖标,李平,郭辉瑞,李平华,鲁顺宝,章荣立,刘肃平.[Co(meamp)(amp)Cl][ZnCl_4]体系配合物一异构体的合成、结构特征与量子化学计算[J].复旦学报(自然科学版),2007,46(3):335-343. 被引量:2
-
3温祖标,郭辉瑞,李平,李平华.[Co(appma)(amp)Cl][ZnCl_4]体系配合物中一面式异构体的晶体结构解析[J].中国科学技术大学学报,2007,37(11):1427-1432.
-
4杨左军,张伟亚,王成云,谢丽琪,蓝芳,潘坤永,吴采樱.溶胶-凝胶富勒烯固相微萃取气相色谱法测定塑料水浸泡液中多种邻苯二甲酸二酯[J].分析化学,2004,32(5):637-640. 被引量:16
-
5罗绪强,陶朱,薛赛凤,祝黔江,张广义,周忠远,周向葛.[Co(ptma)(amp)Cl]^(2+)体系的一反式经式异构体(m3[ZnCl_(4)]·0.5H_(2)O)的晶体结构[J].无机化学学报,2002,18(3):259-264. 被引量:5
-
6陈世平,罗绪强,马培华,林榕光,温祖标,陶朱.[Co(pema)(amp)Cl]^(2+)体系配合物的合成分离[J].贵州大学学报(自然科学版),2005,22(3):305-309.
-
7温祖标,刘超,鲁顺保,郭辉瑞.[Co(bamp)(aep)Cl]^(2+)体系2个几何异构体的理论研究[J].复旦学报(自然科学版),2009,48(1):18-23.
-
8祝黔江,陶朱,张建新,张广义,罗绪强,周忠远,周向葛.[Co(pema)(amp)Cl]^(2+)体系一面式异构体的结构解析及其优势构型[J].化学学报,2003,61(5):729-735. 被引量:8
-
9林榕光,陶朱,张建新,魏赞斌.[Co(pdmma)(ampy)Cl]^(2+)体系——面式异构体的结构解析及其优势构型[J].分子科学学报,2006,22(3):193-199. 被引量:3
-
10沈家庭,易飞,温祖标.[Co(meapma)(amp)Cl]^(2+)体系配合物三异构体的水解合成,结构特性与量子化学计算[J].复旦学报(自然科学版),2011,50(2):158-165.