光诱导合成全氟溴癸烷

Synthesis of Perfluorodecyl Bromide by Photo-induced Method

采用光诱导法合成了人造血液的稳定剂全氟溴癸烷,考察了光源、温度、滴溴速度、反应时间等对反应转化率的影响。对粗产品进行低温精制,得到的产品符合药品的纯度要求。

Perfluorodecyl bromide, an important stabilizer of blood substitute, was synthesized by the advanced photoinduced method. Several important factors during the process, such as light intensity, reaction temperature. The rate of adding bromine, were observed. The crude product was purified at low temperature without further rectification. The product can be used as a composition of medicine.