妇炎康胶囊定性定量方法的研究

Study on identification and determination method for Fuyankang Capsules

目的 :制定妇炎康胶囊的质量标准。方法 :采用薄层色谱法对处方中香附、赤芍、桂枝、黄芪进行定性鉴别 ;用薄层扫描法测定延胡索乙素的含量。结果 :在TLC色谱中均能检出香附、赤芍、桂枝、黄芪 ;延胡索乙素在0 92～ 4 6 30 μg范围呈良好的线性关系 ,r=0 9993,平均回收率 98 86 % ,RSD3 4 %。妇炎康胶囊样品中延胡索乙素含量为 0 17mg g。结论 :所建立的方法可靠 ,能准确地进行定性、定量检测 。

Objective:To establish the quality standards for Fuyan kang Capsules Methods:Rhizoma Cyperi?Rhizoma Corydalis?Radix paeoniae Rubra?Ramulus cinnamomi?Radix Astragali were identified by TLC,and the content of Tetrahydropalmatine by TLC scanning Results: Rhizoma Cyperi?Rhizoma Corydalis?Radix paeoniae Rubra?Ramulus cinnamomi?Radix Astragali could be identified by TLC, Tetrahydropalmatine showed a good linear relationship at a rang of 0 926～4 630 ug, r=0 9993 The average recovery was 98 8%,and RSD was 3 4% The content of Tetrahydropalmatine in Fuyankang Capsules is 0 17mg/g Conclusion:The wethods are accurate and can be used for the qualigy control of Fuyankan Capsules