摘要
利用相转移催化剂四丁基碘化铵(TBAB)催化合成乙酸异丙酯,最佳反应条件如下:催化剂用量0.38 g/0.1 mol乙酸,醇酸比1:2,反应时间1 h,收率87.2％.实验证明,相转移催化对该酯化反应是高效、低成本和实用的合成方法。
Use of TBAB as phase trasfer catalyst on the estcrification of isopropyl acetate was studied. The optimized conditions are as following: the weight of catalyst is 0. 38 g/0. 1 mol acetic acid, the mole ratio of alchol to acid is 1 : 2 and the reaction time is 1h. The chemical yield was87. 2%. Experiment results showed that phase transfer catalyst (TBAB) is a highly active catalyst for this reaction. It is an inexpensive and very practical method.
出处
《哈尔滨师范大学自然科学学报》
CAS
2003年第1期56-58,共3页
Natural Science Journal of Harbin Normal University
