摘要
以氯代叔丁烷和异丁醛为原料 ,通过格氏试剂法合成了 2 ,2 ,4 三甲基 3 戊醇 ,研究了溶剂种类与用量、滴加时间、反应时间等因素对收率的影响及其规律 。
2,2,4-Trimethylpentan 3 ol were synthesized by the Grignard reaction from 2 chloro 2 methylpropane and isobutyraldehyde. The effects of the species and amount of solvents, dropping and reaction time were studied in particular. The optimum reaction conditions were presented.
出处
《合成化学》
CAS
CSCD
2003年第2期153-155,162,共4页
Chinese Journal of Synthetic Chemistry
基金
黑龙江省自然科学基金资助项目 (B0 1-0 7)
关键词
氯代叔丁烷
异丁醛
2
2
4-三甲基-3-戊醇
合成
格氏试剂法
lipophilic metal phthalocyanine
2,2,4 trimethylpentan 3 ol
Grignard reaction
isobutyraldehyde
chloromethypropane
synthesis
