二(3-腈基乙基)氨基乙腈的合成及表征

The Synthesis and Characterization of Bi(3-nitrilethylene) Aminoacetonitrile

由氨基乙腈和丙烯腈进行加成反应合成一种新化合物二(3-腈基乙基)氨基乙腈,用红外光谱、1HNMR核磁共振谱、元素分析、热重分析对其结构和热性质进行了表征。结果证实所制备的化合物即为目标化合物,该化合物在300℃以下具有较好的热稳定性。

A new compound bi(3nitrilethylene) aminoacetonitrile was synthesized by the reaction of aminoacetonitrile and acrylonitrile. It was characterized by IR spectrum, 1H NMR, TGDTA and elemental analysis. The result indicated that the compound synthesized is really the objective compound, and the compound has high stability under the temperature of 300 ℃.