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微波辐射法合成丙二酸甲(乙)烷酯 被引量:1

Synthesis of alkyl methyl(ethyl) malonates under microwave irradiation
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摘要 Alkyl methyl(ethyl) malonates were synthesized by solidliquid phase transfer catalysis without solvent in the new method of the reaction of potassium methyl(ethyl) malonate with alkyl bromide or chloride with high yields.Under the microwave irradiation,the reaction time was reduced from 2h to 2min with equal yield. Alkyl methyl(ethyl) malonates were synthesized by solidliquid phase transfer catalysis without solvent in the new method of the reaction of potassium methyl(ethyl) malonate with alkyl bromide or chloride with high yields.Under the microwave irradiation,the reaction time was reduced from 2h to 2min with equal yield.
出处 《化学研究与应用》 CAS CSCD 北大核心 2003年第2期233-234,共2页 Chemical Research and Application
关键词 微波辐射法 合成 丙二酸甲烷酯 丙二酸乙烷酯 固液相转移催化 alkyl methyl(ethyl) malonates synthesis solid-liquid phase transfer catalysis microwave
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