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微波法固相合成二茂铁基α、β-不饱和酮 被引量:6

Microwave-assisted synthesis of ferrocenyl α,β-unsaturated ketones in solid phase
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摘要 Microwave irradiation can accelerate the rate of the synthesis reaction of ferrocenyl α,β unsaturated ketones by using KF Al 2O 3 as a catalyst. Six fitled compounds were prepared with microware assisted synthesis. Their structures were characterized by 1H NMR, IR, and elemental analysis. Microwave irradiation can accelerate the rate of the synthesis reaction of ferrocenyl α,β unsaturated ketones by using KF Al 2O 3 as a catalyst. Six fitled compounds were prepared with microware assisted synthesis. Their structures were characterized by 1H NMR, IR, and elemental analysis.
作者 陆军 陈维一
出处 《化学研究与应用》 CAS CSCD 北大核心 2003年第2期265-266,F003,共3页 Chemical Research and Application
关键词 微波法 固相合成 二茂铁基α β-不饱和酮 氧化铝 氟化钾 固体碱催化剂 ferrocene microwave irradiation KF- Al _2O_3 solid phase
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  • 1Hauser C R,Lindsay J K. J. Journal of Organometallic Chemistry . 1957
  • 2Bublitz D E,Mcewen W E,Kleinberg. J. Journal of the American Chemical Society . 1962
  • 3Lindsay J K,Hauser C R,J. Journal of Organometallic Chemistry . 1957
  • 4ShigaM,KonoH,MotoyamaI,etal. Bull.Chem.Soc.Jpn . 1968

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