卤代硝基三苯醚的合成研究

The Synthesis of Halogenated Nitrotriphenyl Ethers

以取代硝基氯苯和卤代羟基二苯醚为原料合成 6个卤代硝基三苯醚类化合物 ,所得的卤代硝基三苯醚均未见文献报道 ,是一类新结构类型的硝基三苯醚化合物 .其结构经红外、质谱和氢核磁共振谱所确认 。

The halogenated nitrotriphenyl ethers are potential bactericide and insecticide, the authors described the synthesis of six compounds with new structures in 65%～83% yield by the reaction of hydroxyl diphenyl ethers with chloronitrobenzene. All the compounds are reported for the first time and their chemical structures have been confirmed by means of their 1H NMR, MS, IR.