贵金属烤瓷合金旧料再利用后金瓷结合性能测试研究

Metal-ceramic bond of reused surplus alloy of a precious metal ceramic alloy

目的 :探讨废旧贵金属烤瓷合金的重复利用对金瓷结合性能的影响。方法 :对照组采用单纯反复重熔利用BioHeradorN金烤瓷合金至第 4代 ,实验组则采用 2 / 3上代废旧料加 1/ 3新合金循环利用至第四代 ,通过剪切试验测试各组各代试样金瓷结合力。结果 :对照组Ⅰ～Ⅳ代剪切强度依次为 ( 47.5 3±2 .0 2 )、( 33.2 3± 2 .0 3)、( 2 5 .0 8± 1.88)、( 14 .61± 1.5 6)MPa ,呈显著下降趋势 (P <0 .0 1) ;实验组Ⅰ～Ⅳ代剪切强度则为 ( 46.81± 1.5 4)、( 41.0 0± 4.5 6)、( 37.2 5± 2 .2 7)、( 33.37± 2 .17)MPa ,比对照组显著提高(P <0 .0 5 ) ,但各代之间仍存在显著性差异 (P <0 .0 1)。结论 :添加 1/ 3新合金循环重复利用废旧合金 ,可明显改善金瓷之间的结合 ,并能达到临床要求 。

objective: To study the metal ceramic bond of reused surplus alloy of a precious metal ceramic alloy. Methods: The samples in control group for reused surplus alloy were treated by only remelting without adding any fresh alloy up to four generations, those in the test group by adding one third fresh alloy in each generation and up to four generations. Metal ceramic bond strength of the samples was surveied by pull shear test. Results: In control group, the pull shear bond strength (MPa) from generation Ⅰto Ⅳcastings was 47.53±2.02, 33.23±2.03, 25.08±1.88 and 14.61±1.56 respectively( P <0.01).In test group, that was 46.81±1.54, 41.00±4.56, 37.25±2.27 and 33.37±2.17 respectively( P <0.01). In the test group, shear bond strength of the samples decreased less following the rising generation than in the control( P <0.05). Conclusion: Reusing the surplus alloy by adding one third fresh alloy may be an effective way in practice and may meet the clinical requirements for metal ceramic bond of the castings .