摘要
[Objectives] To determine 29 kinds of inorganic elements in samples of Paris daliensis H.Li et V.G.Souku and P. dulongensis H.Li et S.Kuritap produced in different regions, and to measure the content of 10 key inorganic elements: chromium(Cr), manganese(Mn), iron(Fe), copper(Cu), mercury(Hg), zinc(Zn), arsenic(As), antimony(Sr), cadmium(Cd) and lead(Pb). [Methods] The wet digestion and technique of inductively coupled plasma optical emission spectrometry(ICP-OES) were employed. [Results] Under the experimental conditions, elements were not related to each other, and many kinds of elements could be measured at the same time; toxic and heavy metals in samples of P. daliensis H.Li et V.G.Souku and P. dulongensis H.Li et S.Kuritap did not exceed the limit; Hg was not detected in all samples. [Conclusions] This method is simple, easy to operate and reproducible. It can be used for the detection of inorganic elements in P. daliensis H.Li et V.G.Souku and P. dulongensis H.Li et S.Kuritap; the heavy metals and Hg of the rhizome meet the requirements of the limit of medicinal materials.
[Objectives] To determine 29 kinds of inorganic elements in samples of Paris daliensis H.Li et V.G.Souku and P. dulongensis H.Li et S.Kuritap produced in different regions, and to measure the content of 10 key inorganic elements: chromium(Cr), manganese(Mn), iron(Fe), copper(Cu), mercury(Hg), zinc(Zn), arsenic(As), antimony(Sr), cadmium(Cd) and lead(Pb). [Methods] The wet digestion and technique of inductively coupled plasma optical emission spectrometry(ICP-OES) were employed. [Results] Under the experimental conditions, elements were not related to each other, and many kinds of elements could be measured at the same time; toxic and heavy metals in samples of P. daliensis H.Li et V.G.Souku and P. dulongensis H.Li et S.Kuritap did not exceed the limit; Hg was not detected in all samples. [Conclusions] This method is simple, easy to operate and reproducible. It can be used for the detection of inorganic elements in P. daliensis H.Li et V.G.Souku and P. dulongensis H.Li et S.Kuritap; the heavy metals and Hg of the rhizome meet the requirements of the limit of medicinal materials.
基金
Supported by The National Key Research and Development Program of China during the 13th Five-Year Plan Period(2018ZX09301060)
Fourth National Survey of Traditional Chinese Medicine Resources Program(2017)
Science and Technology Condition Capacity Building and Technology Extension Demonstration Project of Aba Prefecture(18TJPT0004)
Innovating Research Program of Postgraduates of Southwest Minzu University in 2019(CX2019SZ180)
