摘要
以碳酸二甲酯为甲基化试剂,在二乙二醇二甲醚溶剂中,进行环戊二烯催化甲基化的研究.通过实验考察反应温度、反应时间、物料配比、催化剂量及碘化钾试剂对甲基环戊二烯产率的影响,确定反应最佳条件,甲基环戊二烯产率达85 8%.
Methylcyclopentadiene(MCPD)was synthesized with dimethyl carbonate and cyclopentadiene.Some influential factors such as ratio of reactant,reaction temperature,reaction time,quantity of sodium and potassium iodide were investigated.The suitable conditions were determined from experimental results.The yield of MCPD reached 85.8%.
出处
《沈阳化工学院学报》
2003年第1期1-3,共3页
Journal of Shenyang Institute of Chemical Technolgy
